2-Amino-4-methyl-6-phenyl-1,3,5-triazine

Base Information

• Chemical Name: 2-Amino-4-methyl-6-phenyl-1,3,5-triazine
• CAS No.: 1853-91-4
• Molecular Formula: C10H10 N4
• Molecular Weight: 186.21
• Hs Code.: 2933699090
• DSSTox Substance ID: DTXSID10274558
• Nikkaji Number: J1.552.691B
• Wikidata: Q82003934
• Mol file: 1853-91-4.mol

Synonyms:1853-91-4;2-Amino-4-methyl-6-phenyl-1,3,5-triazine;4-methyl-6-phenyl-1,3,5-triazin-2-amine;SCHEMBL1131125;DTXSID10274558;AKOS013180690;SB73452;FT-0751969

Chemical Property of 2-Amino-4-methyl-6-phenyl-1,3,5-triazine

Chemical Property:

• Vapor Pressure: 8.56E-08mmHg at 25°C
• Boiling Point: 435.7°C at 760 mmHg
• Flash Point: 247.3°C
• PSA: 64.69000
• Density: 1.217g/cm³
• LogP: 2.01040
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 186.090546336
• Heavy Atom Count: 14
• Complexity: 179

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-AMINO-4-METHYL-6-PHENYL-1,3,5-TRIAZINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=NC(=NC(=N1)N)C2=CC=CC=C2

Technology Process of 2-Amino-4-methyl-6-phenyl-1,3,5-triazine

There total 2 articles about 2-Amino-4-methyl-6-phenyl-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

N,N-dimethyl acetamide (127-19-5,116057-81-9) + guanidine hydrochloride (50-01-1) + ethyl benzimidate hydrochloride (5333-86-8) → 4-methyl-6-phenyl-1,3,5-triazin-2-amine (1853-91-4)

Guidance literature:

With caesium carbonate; at 150 ℃; for 24h; under 760.051 Torr; Reagent/catalyst; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.joc.7b01510

Reference yield:

→ 4-methyl-6-phenyl-1,3,5-triazin-2-amine (1853-91-4)

Guidance literature:

Benzamidinhydrochlorid u. N-Cyan-acetamidin, (150grad, 3h),Ausb. 26percent;

DOI:10.1021/jo01042a017

upstream raw materials:

N,N-dimethyl acetamide

guanidine hydrochloride

ethyl benzimidate hydrochloride

Refernces

• 1、 -. "Process for the preparation of 2-amino-s-triazines". . . Retrieved 2008/06/13.