4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

Base Information

Chemical Name:4,4'-dinitro-4''-N-phenothiazinyltriphenylamine
CAS No.:1257518-45-8
Molecular Formula:C₃₀H₂₀N₄O₄S
Molecular Weight:532.579
Hs Code.:

Synonyms:4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

Chemical Property:

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Technology Process of 4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

There total 3 articles about 4,4'-dinitro-4''-N-phenothiazinyltriphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 19606-95-2
10-(4-aminophenyl)-10-H-phenothiazine

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1257518-45-8
4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

Guidance literature:: With cesium fluoride; In dimethyl sulfoxide; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c0jm01889a

Reference yield:

: 92-84-2
10H-phenothiazine

: 1257518-45-8
4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 9 h / Inert atmosphere; Reflux

3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrazine hydrate; cesium fluoride; In ethanol; dimethyl sulfoxide;
DOI:10.1039/c0jm01889a

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1257518-45-8
4,4'-dinitro-4''-N-phenothiazinyltriphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 9 h / Inert atmosphere; Reflux

3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrazine hydrate; cesium fluoride; In ethanol; dimethyl sulfoxide;
DOI:10.1039/c0jm01889a