1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

Base Information

Chemical Name:1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane
CAS No.:713090-40-5
Molecular Formula:C₁₈H₂₅Br₂NO₄
Molecular Weight:479.209
Hs Code.:

Synonyms:1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

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Chemical Property of 1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

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Technology Process of 1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

There total 2 articles about 1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 558-13-4
carbon tetrabromide

: 66749-96-0
4-(1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl)-benzaldehyde

: 603-35-0
triphenylphosphine

: 713090-40-5
1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

Guidance literature:: carbon tetrabromide; triphenylphosphine; With zinc; In dichloromethane; at -15 - 20 ℃; for 3.5h;

4-(1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl)-benzaldehyde; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/b401092b

Reference yield:

: 66750-10-5
13-phenyl-1,4,7,10-tetraoxa-13-aza-cyclopentadecane

: 713090-40-5
1-[4-(2,2-dibromovinyl)phenyl]4,7,10,13-tetraoxa-1-azacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Zn / CH₂Cl₂ / 3.5 h / -15 - 20 °C

1.2: 24 percent / CH₂Cl₂ / 2 h / 20 °C

With zinc; In dichloromethane; 1.1: Vilsmeyer reaction / 2.1: Corey-Fuchs method / 2.2: Wittig reaction;
DOI:10.1039/b401092b