1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

Base Information

• Chemical Name: 1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene
• CAS No.: 405316-54-3
• Molecular Formula: C₇₆H₉₂O₄
• Molecular Weight: 1069.56
• Mol file: 405316-54-3.mol

Synonyms:1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

Chemical Property of 1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

There total 1 articles about 1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,6,7,12-tetrakis(4'(1,1,3,3-tetramethylbutyl)phenoxy)3,4,9,10-perylene tetracarboxylic dianhydride (262360-46-3) → 1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene (405316-54-3)

Guidance literature:

With copper(I) oxide; copper; In quinoline; at 220 ℃; for 8h;

DOI:10.1021/ma011724d

Reference yield: 47.0%

1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene (405316-54-3) → 3,10-dibromo-1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene + 3,9-dibromo-1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1021/ma011724d

Reference yield:

1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene (405316-54-3) → 3-bromo-1,6,7,12-tetrakis-[4-(1,1,3,3-tetramethyl-butyl)-phenoxy]-perylene + 3,10-dibromo-1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene + 3,9-dibromo-1,6,7,12-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]perylene

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 70 ℃; for 24h; Title compound not separated from byproducts;

DOI:10.1021/ma011724d

upstream raw materials:

1,6,7,12-tetrakis(4'(1,1,3,3-tetramethylbutyl)phenoxy)3,4,9,10-perylene tetracarboxylic dianhydride