[5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II)

Base Information

• Chemical Name: [5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II)
• CAS No.: 1548823-41-1
• Molecular Formula: C₆₂H₇₀I₂N₄Ni
• Molecular Weight: 1183.76

Synonyms:[5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II)

Chemical Property of [5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II)

Chemical Property:

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Technology Process of [5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II)

There total 1 articles about [5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-iodo-succinimide (516-12-1) + 5,10,15-triaryl-2,18-diborylporphyrin nickel(II) complex (942588-55-8) → [5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II) (1548823-41-1)

Guidance literature:

With copper(l) iodide; In N,N-dimethyl-formamide; toluene; at 80 ℃; for 3h;

DOI:10.1021/ol501448r

Reference yield: 98.0%

[5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II) (1548823-41-1) → Ni(II) 5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-dideuteroporphyrin

Guidance literature:

[5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II); With n-butyllithium; In tetrahydrofuran; hexane; at -98 ℃; for 0.5h; Inert atmosphere;

With water-d2; In tetrahydrofuran; hexane;

DOI:10.1002/chem.201502563

Reference yield: 90.0%

[5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-diiodoporphyrinato]nickel(II) (1548823-41-1) + sodium thiophenolate (930-69-8) → 5,10,15-tris(3,5-di-tert-butylphenyl)-2,18-bis(phenylthio)porphyrinatonickel(II)

Guidance literature:

In N,N-dimethyl-formamide; at 110 ℃;

DOI:10.1016/j.cclet.2021.02.022

upstream raw materials:

N-iodo-succinimide

5,10,15-triaryl-2,18-diborylporphyrin nickel(II) complex

Downstream raw materials:

C₇₀H₈₆N₆O₂Zn

C₇₄H₈₂N₆Zn

C₇₆H₈₄N₄S₂Zn

C₆₂H₇₀I₂N₄Zn

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