2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol

Base Information

• Chemical Name: 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol
• CAS No.: 185450-10-6
• Molecular Formula: C₂₆H₃₆N₆O₈
• Molecular Weight: 560.607

Synonyms:2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol

Chemical Property of 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol

There total 2 articles about 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-diazido-3,4-O-isopropylidene-1,6-di-O-phenyl-2,5-dideoxy-D-iditol (185450-05-9) → 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol (185450-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 3M HCl / acetonitrile / 4 h / 50 °C

2: 1.) NaH / 1.) THF, 15 min, 2.) THF, overnight

With hydrogenchloride; sodium hydride; In acetonitrile;

DOI:10.1021/jm960728j

Reference yield:

2-Methoxyethoxymethyl chloride (3970-21-6) + 2,5-diazido-1,6-di-O-phenyl-2,5-dideoxy-D-iditol (185450-07-1) → 2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol (185450-10-6)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, 15 min, 2.) THF, overnight;

DOI:10.1021/jm960728j

Reference yield:

2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol (185450-10-6) → (2R,3S,4S,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-1,6-diphenoxy-hexane-2,5-diamine (1053613-76-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/jm960728j

upstream raw materials:

2-Methoxyethoxymethyl chloride

2,5-diazido-1,6-di-O-phenyl-2,5-dideoxy-D-iditol

2,5-diazido-3,4-O-isopropylidene-1,6-di-O-phenyl-2,5-dideoxy-D-iditol

Downstream raw materials:

(2R,3S,4S,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-1,6-diphenoxy-hexane-2,5-diamine

(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

(4R,5S,6S,7R)-1,3-Bis-(4-hydroxymethyl-benzyl)-5,6-bis-(2-methoxy-ethoxymethoxy)-4,7-bis-phenoxymethyl-[1,3]diazepan-2-one

(3R,4S,5S,6R)-2,7-Dibenzyl-4,5-bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

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