(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Base Information

Chemical Name:(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide
CAS No.:185450-20-8
Molecular Formula:C₂₆H₃₈N₂O₁₀S
Molecular Weight:570.661
Hs Code.:

Synonyms:(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Suppliers and Price of (3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

There total 3 articles about (3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 185450-10-6
2,5-diazido-3,4-bis-O-[(2-methoxyethoxy)methyl]-1,6-di-O-phenyl-2,5-dideoxy-d-iditol

: 185450-20-8
(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate

2: sulfamide / pyridine / 16 h / Heating

With hydrogen; SULFAMIDE; palladium on activated charcoal; In pyridine; ethyl acetate;
DOI:10.1021/jm960728j

Reference yield:

: 185450-07-1
2,5-diazido-1,6-di-O-phenyl-2,5-dideoxy-D-iditol

: 185450-20-8
(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 15 min, 2.) THF, overnight

2: H₂ / 10percent Pd/C / ethyl acetate

3: sulfamide / pyridine / 16 h / Heating

With hydrogen; sodium hydride; SULFAMIDE; palladium on activated charcoal; In pyridine; ethyl acetate;
DOI:10.1021/jm960728j

Reference yield:

: 185450-05-9
2,5-diazido-3,4-O-isopropylidene-1,6-di-O-phenyl-2,5-dideoxy-D-iditol

: 185450-20-8
(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / 3M HCl / acetonitrile / 4 h / 50 °C

2: 1.) NaH / 1.) THF, 15 min, 2.) THF, overnight

3: H₂ / 10percent Pd/C / ethyl acetate

4: sulfamide / pyridine / 16 h / Heating

With hydrogenchloride; hydrogen; sodium hydride; SULFAMIDE; palladium on activated charcoal; In pyridine; ethyl acetate; acetonitrile;
DOI:10.1021/jm960728j