4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

Base Information

Chemical Name:4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide
CAS No.:1609945-64-3
Molecular Formula:C₂₇H₃₄N₄O
Molecular Weight:430.593
Hs Code.:

Synonyms:4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

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Chemical Property of 4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

Chemical Property:

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Technology Process of 4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

There total 5 articles about 4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2438-05-3
4-n-propylbenzoic acid

: N-propyl-N,N'-bis-(pyridine-2-ylmethyl)ethane-1,2-diamine

: 1609945-64-3
4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

Guidance literature:: 4-n-propylbenzoic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.166667h;

N-propyl-N,N'-bis-(pyridine-2-ylmethyl)ethane-1,2-diamine; In dichloromethane; at 20 ℃;
DOI:10.1002/chem.201302708

Reference yield:

: tert-butyl 2-(propyl(pyridine-2-ylmethyl)amino)ethylcarbamate

: 1609945-64-3
4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 2 h / 20 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1.5 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.17 h

3.2: 20 °C

With sodium tris(acetoxy)borohydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201302708

Reference yield:

: 294646-09-6
{2-[(pyridin-2-ylmethyl)amino]ethyl}carbamic acid tert-butyl ester

: 1609945-64-3
4-propyl-N-[2-(propylpyridine-2-ylmethylamino)ethyl]-N-pyridine-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / Reflux

2.1: dichloromethane / 2 h / 20 °C

3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.17 h

4.2: 20 °C

With sodium tris(acetoxy)borohydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1002/chem.201302708