1-nitro-1-nitrosocyclohexane

Base Information

• Chemical Name: 1-nitro-1-nitrosocyclohexane
• CAS No.: 14296-14-1
• Molecular Formula: C6H10 N2 O3
• Molecular Weight: 158.157
• Mol file: 14296-14-1.mol

Synonyms:1-Nitro-1-nitrosocyclohexane

Chemical Property of 1-nitro-1-nitrosocyclohexane

Chemical Property:

• Vapor Pressure: 0.0223mmHg at 25°C
• Boiling Point: 250°Cat760mmHg
• Flash Point: 105°C
• PSA: 75.25000
• Density: 1.39g/cm³
• LogP: 2.21310

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-nitro-1-nitrosocyclohexane

There total 5 articles about 1-nitro-1-nitrosocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-nitrocyclohexane (1122-60-7) → gem-nitrosocyclohexane pseudonitrol (14296-14-1)

Guidance literature:

With cis-nitrous acid;

Reference yield:

nitrocyclohexane potassium salt (3424-17-7,12385-03-4) → gem-nitrosocyclohexane pseudonitrol (14296-14-1)

Guidance literature:

With nitrosonium perchlorate; In acetonitrile; at 25 ℃; Thermodynamic data; Inert atmosphere;

DOI:10.1021/jo900732b

Reference yield:

1-Bromo-1-nitroso-cyclohexane → gem-nitrosocyclohexane pseudonitrol (14296-14-1)

Guidance literature:

With silver(I) nitrite;

upstream raw materials:

1-nitrocyclohexane

cis-nitrous acid

cyclohexane

nitrocyclohexane potassium salt

Downstream raw materials:

1-bromo-1-nitrocyclohexane

Adipic acid

1,1-dinitrocyclohexane

4-nitro-3-(1-nitrocyclohex-1-yl-ONN-azoxy)furazan

Refernces