phenylmethyldimethoxyphosphonium trifluoromethanesulfonate

Base Information

• Chemical Name: phenylmethyldimethoxyphosphonium trifluoromethanesulfonate
• CAS No.: 64294-67-3
• Molecular Formula: CF₃O₃S*C₉H₁₄O₂P
• Molecular Weight: 334.253
• Mol file: 64294-67-3.mol

Synonyms:phenylmethyldimethoxyphosphonium trifluoromethanesulfonate

Chemical Property of phenylmethyldimethoxyphosphonium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of phenylmethyldimethoxyphosphonium trifluoromethanesulfonate

There total 3 articles about phenylmethyldimethoxyphosphonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl methylphenylphosphinate (6389-79-3) + methyl trifluoromethanesulfonate (333-27-7) → phenylmethyldimethoxyphosphonium trifluoromethanesulfonate (64294-67-3)

Guidance literature:

In dichloromethane; Ambient temperature;

DOI:10.1021/ja00304a029

Reference yield:

Dichlorophenylphosphine (644-97-3) → phenylmethyldimethoxyphosphonium trifluoromethanesulfonate (64294-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1: PhNEt₂ / diethyl ether

2: diethyl ether

With N,N-diethylaniline; In diethyl ether;

DOI:10.1021/jo00398a010

Reference yield:

phenylphosphonous acid dimethyl ester (2946-61-4) + methyl trifluoromethanesulfonate (333-27-7) → phenylmethyldimethoxyphosphonium trifluoromethanesulfonate (64294-67-3)

Guidance literature:

In diethyl ether;

DOI:10.1021/jo00398a010

upstream raw materials:

phenylphosphonous acid dimethyl ester

methyl trifluoromethanesulfonate

methyl methylphenylphosphinate

Dichlorophenylphosphine

Downstream raw materials:

methyl methylphenylphosphinate

2,4-dinitroanisole

Refernces