2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

Base Information

Chemical Name:2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside
CAS No.:149831-86-7
Molecular Formula:C₄₉H₅₀N₂O₉S
Molecular Weight:843.01
Hs Code.:

Synonyms:2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

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Chemical Property of 2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

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Technology Process of 2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

There total 11 articles about 2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149831-85-6
2-(N-(phenylsulfonyl)indol-3-yl)ethyl 3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

: 149831-86-7
2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 4h; Yield given; Heating;

Reference yield:

: 526-55-6,930395-07-6
2-(3-indole)-ethanol

: 149831-86-7
2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

2: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 16 h

3: 84 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / Ambient temperature

4: ZnCl₂ / tetrahydrofuran; diethyl ether / 1 h / -78 °C

5: AIBN, tributyltin hydride / toluene / 4 h / Heating

With 1H-imidazole; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; zinc(II) chloride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 149831-86-7
2-(N-(phenylsulfonyl)indol-3-yl)ethyl 2-deoxy-3,4-di-O-benzyl-6-O-(5-phthalimidopentyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / benzene / 5 h / Ambient temperature

2: 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 0.17 h / Ambient temperature

3: NaH, 15-crown-5 / CH₂Cl₂ / 24 h / Ambient temperature

4: dimethyldioxirane / acetone; CH₂Cl₂ / 1 h / 0 °C

5: ZnCl₂ / tetrahydrofuran; diethyl ether / 1 h / -78 °C

6: AIBN, tributyltin hydride / toluene / 4 h / Heating

With 2,6-di-tert-butyl-4-methylpyridine; 15-crown-5; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3,3-dimethyldioxirane; sodium hydride; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene; benzene;