(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Base Information

Chemical Name:(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate
CAS No.:122037-30-3
Molecular Formula:C₂₉H₂₄Cl₃NO₈
Molecular Weight:620.87
Hs Code.:

Synonyms:(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

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Chemical Property of (2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

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Technology Process of (2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

There total 8 articles about (2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1146468-69-0
2,3,4-Tri-O-benzoyl-6-desoxy-α,β-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 122037-30-3
(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: With 1,5-Diazabicyclo[5.4.0]undec-5-ene; In dichloromethane; for 3h; Ambient temperature;

Reference yield: 78.0%

: 1146468-69-0
2,3,4-Tri-O-benzoyl-6-desoxy-α,β-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: C₂₉H₂₄Cl₃NO₈

: 122037-30-3
(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: With caesium carbonate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1248/cpb.c20-00834

Reference yield:

: 141020-07-7
1-O-Acetyl-2,3,4-tri-O-benzoyl-6-desoxy-α-D-galactopyranose

: 122037-30-3
(2R,3S,4S,5R,6R)-2-methyl-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / piperidine / tetrahydrofuran / 18 h / Ambient temperature

2: 95 percent / 1,5-diazabocyclo<5.4.0>undec-5-ene / CH₂Cl₂ / 3 h / Ambient temperature

With piperidine; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In tetrahydrofuran; dichloromethane;