3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

Base Information

Chemical Name:3-(2-methylphenyl)-4,5-dimethylthiazolium chloride
CAS No.:1010456-80-0
Molecular Formula:C₁₂H₁₄NS*Cl
Molecular Weight:239.769
Hs Code.:

Synonyms:3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

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Chemical Property of 3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

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Technology Process of 3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

There total 1 articles about 3-(2-methylphenyl)-4,5-dimethylthiazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 94-69-9
2'-methylformanilide

: 4091-39-8
3-chloro-2-butanone

: 1010456-80-0
3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

Guidance literature:: 2'-methylformanilide; With tetraphosphorus decasulfide; In 1,4-dioxane; at 20 ℃;

3-chloro-2-butanone; In 1,4-dioxane; Further stages.; Heating;
DOI:10.1021/ja075849v

Reference yield: 53.0%

: Hoveyda-Grubbs catalyst first generation

: 1010456-80-0
3-(2-methylphenyl)-4,5-dimethylthiazolium chloride

: [RuCl₂(3-(2-methylphenyl)-4,5-dimethylthiazol-2-ylidene)(=CH-o-iPrO-Ph)]

Guidance literature:: With silver(l) oxide; In dichloromethane; (Ar); ligand salt, Ag2O and molecular sieves suspended in CH2Cl2, stirred at room temp., Ru complex added, stirred under N2 at room temp. in thedark; evapd. (vac.), dissolved in C6H6, chromd. (silica gel, pentanes/Et2O), evapd. (vac.), dissolved in C6H6, lyophilized;
DOI:10.1021/ja075849v