Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)-

Base Information

• Chemical Name: Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)-
• CAS No.: 2151-17-9
• Molecular Formula: C17H17ClO6
• Molecular Weight: 352.771
• DSSTox Substance ID: DTXSID40175847
• Wikidata: Q83046177
• Mol file: 2151-17-9.mol

Synonyms:2151-17-9;Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)-;(3-chloro-2-hydroxy-4,6-dimethoxyphenyl)-(4-hydroxy-2-methoxy-6-methylphenyl)methanone;(3-Chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)methanone;DTXSID40175847

Chemical Property of Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)-

Chemical Property:

• Vapor Pressure: 1.83E-14mmHg at 25°C
• Melting Point: 213-214°C
• Boiling Point: 588.9°Cat760mmHg
• Flash Point: 309.9°C
• PSA: 85.22000
• Density: 1.333g/cm³
• LogP: 3.31640
• XLogP3: 4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 352.0713660
• Heavy Atom Count: 24
• Complexity: 433

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC(=CC(=C1C(=O)C2=C(C(=C(C=C2OC)OC)Cl)O)OC)O

Technology Process of Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)-

There total 7 articles about Methanone, (3-chloro-2-hydroxy-4,6-dimethoxyphenyl)(4-hydroxy-2-methoxy-6-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-dehydrogriseofulvin (69744-08-7) → 3-chloro-2,2'-dihydroxy-6'-methyl-2',4,6-trimethoxybenzophenone (2151-17-9) + (+)-dihydrogriseofulvin (17793-63-4,17793-64-5,86594-40-3,86594-41-4,86594-43-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 5h;

DOI:10.1248/cpb.31.934

Reference yield:

(+/-)-dehydrogriseofulvin (7776-77-4) → 3-chloro-2,2'-dihydroxy-6'-methyl-2',4,6-trimethoxybenzophenone (2151-17-9) + (+)-dihydrogriseofulvin (17793-63-4,17793-64-5,86594-40-3,86594-41-4,86594-43-6) + (-)-griseofulvin (126-07-8,469-49-8,1588-01-8,2884-22-2,6915-11-3,67890-77-1,78739-00-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 1.5h; Ambient temperature;

DOI:10.1248/cpb.29.2313

Reference yield:

→ 3-chloro-2,2'-dihydroxy-6'-methyl-2',4,6-trimethoxybenzophenone (2151-17-9)

Guidance literature:

With palladium on activated charcoal; ethanol; Hydrogenation;

upstream raw materials:

(+)-dehydrogriseofulvin

(+/-)-dehydrogriseofulvin

ethanol

(-)-dehydrogriseofulvin

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