estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl

Base Information

• Chemical Name: estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl
• CAS No.: 1166993-64-1
• Molecular Formula: C₈₃H₉₈N₁₆O₂₀
• Molecular Weight: 1639.79

Synonyms:estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl

Chemical Property of estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl

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Technology Process of estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl

There total 1 articles about estrone-3-O-methylcarbonyl-Arg(NO₂)-Gly-Asp(Bzl)-Phe-Arg(NO₂)-Gly-Asp(Bzl)-Phe-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-OBn hydrochloride (1147834-49-8) + 2-(((8R,9S,13S,14S)-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl)oxy)acetic acid (1428-66-6) → estrone-3-O-methylcarbonyl-Arg(NO2)-Gly-Asp(Bzl)-Phe-Arg(NO2)-Gly-Asp(Bzl)-Phe-OBzl (1166993-64-1)

Guidance literature:

2-(((8R,9S,13S,14S)-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl)oxy)acetic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-OBn hydrochloride; With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃; pH=8.5; Inert atmosphere;

DOI:10.1016/j.bmc.2009.03.057

Reference yield: 71.0%

estrone-3-O-methylcarbonyl-Arg(NO2)-Gly-Asp(Bzl)-Phe-Arg(NO2)-Gly-Asp(Bzl)-Phe-OBzl (1166993-64-1) → estrone-3-O-methylcarbonyl-Arg-Gly-Asp-Phe-Arg-Gly-Asp-Phe (1166993-87-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; water; for 20h; Inert atmosphere;

DOI:10.1016/j.bmc.2009.03.057

upstream raw materials:

Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-Arg(Nω-NO2)-Gly-Asp(OBn)-Phe-OBn hydrochloride

2-(((8R,9S,13S,14S)-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl)oxy)acetic acid

Downstream raw materials:

estrone-3-O-methylcarbonyl-Arg-Gly-Asp-Phe-Arg-Gly-Asp-Phe

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