4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Base Information

• Chemical Name: 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine
• CAS No.: 1207449-52-2
• Molecular Formula: C₁₅H₁₈ClN₅O₃
• Molecular Weight: 351.793

Synonyms:4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Chemical Property of 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

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Technology Process of 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

There total 1 articles about 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

2,6-Dichloro-4-morpholino-1,3,5-triazine (6601-22-5) + 3.5-dimethoxyaniline (10272-07-8) → 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine (1207449-52-2)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1002/hlca.201200015

Reference yield: 23.0%

4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine (1207449-52-2) + ethylenediamine (107-15-3,85404-18-8) → N-(2-aminoethyl)-N'-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazine-2,4-diamine (1393922-30-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 - 60 ℃; for 3h;

DOI:10.1002/hlca.201200015

Reference yield:

N-(7-chloroquinolin-4-yl)ethylenediamine (5407-57-8) + 4-chloro-N-(3,5-dimethoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine (1207449-52-2) → N-[2-(7-chloro-quinolin-4-ylamino)-ethyl]-N'-(3,5-dimethoxy-phenyl)-6-morpholin-4-yl-[1,3,5]triazine-2,4-diamine (1207449-55-5)

Guidance literature:

With potassium carbonate; In acetonitrile; at 82 ℃;

DOI:10.1016/j.bmcl.2009.10.106

upstream raw materials:

2,6-Dichloro-4-morpholino-1,3,5-triazine

3.5-dimethoxyaniline

Downstream raw materials:

N-[2-(7-chloro-quinolin-4-ylamino)-ethyl]-N'-(3,5-dimethoxy-phenyl)-6-morpholin-4-yl-[1,3,5]triazine-2,4-diamine

C₂₇H₃₁ClN₈O₃

C₃₀H₃₇ClN₈O₃

C₂₈H₃₃ClN₈O₃

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