[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

Base Information

Chemical Name:[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone
CAS No.:1243484-35-6
Molecular Formula:C₁₈H₁₆N₂O₂S
Molecular Weight:324.403
Hs Code.:

Synonyms:[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

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Technology Process of [4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

There total 3 articles about [4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 95-16-9
1,3-Benzothiazole

: 79271-22-0
4-(4-Iodobenzoyl)morpholine

: 1243484-35-6
[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

Guidance literature:: With [2,2]bipyridinyl; nickel(II) acetate tetrahydrate; lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 36h; Inert atmosphere;
DOI:10.1002/chem.201101091

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1243484-35-6
[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 7 h / 80 °C / Inert atmosphere

2: 5 h / 0 - 20 °C / Inert atmosphere

3: [2,2]bipyridinyl; nickel(II) acetate tetrahydrate; lithium tert-butoxide / 1,4-dioxane / 36 h / 120 °C / Inert atmosphere

With [2,2]bipyridinyl; thionyl chloride; nickel(II) acetate tetrahydrate; lithium tert-butoxide; In 1,4-dioxane;
DOI:10.1002/chem.201101091

Reference yield:

: 1711-02-0
4-iodobenzoic acid chloride

: 1243484-35-6
[4-(2-benzothiazolyl)phenyl]-4-morpholinylmethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 5 h / 0 - 20 °C / Inert atmosphere

2: [2,2]bipyridinyl; nickel(II) acetate tetrahydrate; lithium tert-butoxide / 1,4-dioxane / 36 h / 120 °C / Inert atmosphere

With [2,2]bipyridinyl; nickel(II) acetate tetrahydrate; lithium tert-butoxide; In 1,4-dioxane;
DOI:10.1002/chem.201101091