Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

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Chemical Name:Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester
CAS No.:375345-63-4
Molecular Formula:C₃₆H₅₂N₈O₇SSi₂
Molecular Weight:797.095
Hs Code.:

Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

Synonyms:Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

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Chemical Property of Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

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Technology Process of Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

There total 6 articles about Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 375345-68-9
N-[6-Dimethylamino-9-((2R,3R,3aS,9aR)-3-hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-9H-purin-2-yl]-2-phenoxy-acetamide

: 375345-63-4
Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 13h;
DOI:10.1246/cl.2001.914

Reference yield:

: 32464-89-4
2-amino-6-(dimethylamino)-9-(β-D-ribofuranosyl)purine

: 375345-63-4
Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 1.5 h / 20 °C

2: 17 h / 20 °C

3: aq. NH₄OH / 0.25 h / 0 °C

4: 94 percent / pyridine / dimethylformamide / 1 h / 20 °C

5: 95 percent / dimethylformamide / 13 h / 20 °C

With pyridine; ammonium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1246/cl.2001.914

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 375345-63-4
Imidazole-1-carbothioic acid O-{(2R,3R,3aR,9aR)-2-[6-dimethylamino-2-(2-phenoxy-acetylamino)-purin-9-yl]-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / pyridine / dimethylformamide / 1 h / 20 °C

2: 95 percent / dimethylformamide / 13 h / 20 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1246/cl.2001.914