N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide
CAS No.:116470-04-3
Molecular Formula:C₁₅H₂₁NO₃S
Molecular Weight:295.403
Hs Code.:

Synonyms:N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

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Chemical Property of N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

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Technology Process of N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

There total 4 articles about N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 116415-21-5
(1R,2S,3S,4S)-3-(Toluene-4-sulfonylamino)-bicyclo[2.2.1]heptane-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 116470-04-3
N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;
DOI:10.1016/S0040-4039(01)81069-8

Reference yield:

: (2S,3S)-3-Isocyanato-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 116470-04-3
N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

2: HCl / Pd/C / methanol

4: 96 percent / LAH / diethyl ether / 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1016/S0040-4039(01)81069-8

Reference yield:

: 116440-64-3
(1S,2S,3S,4R)-3-Benzyloxycarbonylamino-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 116470-04-3
N-((1S,2S,3S,4R)-3-Hydroxymethyl-bicyclo[2.2.1]hept-2-yl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / Pd/C / methanol

3: 96 percent / LAH / diethyl ether / 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1016/S0040-4039(01)81069-8