Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate

Base Information

Chemical Name:Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate
CAS No.:6304-69-4
Molecular Formula:C20H30N4O8
Molecular Weight:454.48
Hs Code.:
NSC Number:42994
DSSTox Substance ID:DTXSID10285846
Wikidata:Q82021368

Synonyms:6304-69-4;tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate;NSC42994;DTXSID10285846;NSC-42994

Suppliers and Price of Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.256g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:10
Exact Mass:454.20636393
Heavy Atom Count:32
Complexity:593

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)NN(C1=CC(=C(C=C1C)N(C(=O)OCC)NC(=O)OCC)C)C(=O)OCC

Technology Process of Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate

There total 2 articles about Tetraethyl 1,1'-(2,5-dimethylbenzene-1,4-diyl)dihydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-42-3
para-xylene

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 338979-43-4
(2,5-dimethyl-phenyl)-hydrazine-N,N'-dicarboxylic acid diethyl ester

: 6304-69-4
(2,5-dimethyl-p-phenylene)-bis-hydrazine-N,N'-dicarboxylic acid tetraethyl ester

Guidance literature:: With sulfuric acid;

Reference yield:

: 106-42-3
para-xylene

: 7664-93-9
sulfuric acid

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 338979-43-4
(2,5-dimethyl-phenyl)-hydrazine-N,N'-dicarboxylic acid diethyl ester

: 6304-69-4
(2,5-dimethyl-p-phenylene)-bis-hydrazine-N,N'-dicarboxylic acid tetraethyl ester

Guidance literature:: at 20 ℃;

Reference yield:

: 6304-69-4
(2,5-dimethyl-p-phenylene)-bis-hydrazine-N,N'-dicarboxylic acid tetraethyl ester

: 79817-50-8
N,N'-dimethyl-N,N'-(2,5-dimethyl-p-phenylene)-bis-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; diethyl ether

2: aqueous HI; phosphorus; acetic acid / anschliessende Reaktion mit Acetanhydrid und Kaliumacetat

With phosphorus; lithium aluminium tetrahydride; diethyl ether; hydrogen iodide; acetic acid;