n-butyl 3-methylamino-4-nitrocinnamate

Base Information

Chemical Name:n-butyl 3-methylamino-4-nitrocinnamate
CAS No.:1370023-74-7
Molecular Formula:C₁₄H₁₈N₂O₄
Molecular Weight:278.308
Hs Code.:

Synonyms:n-butyl 3-methylamino-4-nitrocinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-butyl 3-methylamino-4-nitrocinnamate

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Technology Process of n-butyl 3-methylamino-4-nitrocinnamate

There total 4 articles about n-butyl 3-methylamino-4-nitrocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 35966-84-8
4-chloro-2-methylaminonitrobenzene

: 1370023-74-7
n-butyl 3-methylamino-4-nitrocinnamate

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; lithium chloride; at 110 ℃; for 12h; Inert atmosphere;

Reference yield: 96.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 67567-44-6
(5-chloro-2-nitrophenyl)-methylamine

: 1370023-74-7
n-butyl 3-methylamino-4-nitrocinnamate

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; lithium chloride; at 110 ℃; for 12h; Inert atmosphere;

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 1370023-74-7
n-butyl 3-methylamino-4-nitrocinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dimethyl sulfoxide / 20 - 35 °C

2: palladium diacetate; lithium chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere

With palladium diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; In N,N-dimethyl acetamide; dimethyl sulfoxide; 2: |Heck Reaction;