(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

Base Information

Chemical Name:(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate
CAS No.:1101134-05-7
Molecular Formula:C₃₀H₃₆O₅Si
Molecular Weight:504.698
Hs Code.:

Synonyms:(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

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Technology Process of (S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

There total 1 articles about (S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1101134-04-6
C₂₃H₃₂O₄Si

: 98-88-4
benzoyl chloride

: 1101134-05-7
(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.028

Reference yield: 100.0%

: 1101134-05-7
(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate

: 1066-54-2
trimethylsilylacetylene

: 1101134-06-8
C₃₅H₄₆O₅Si₂

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

(S)-2-[3-(tert-butyldiphenylsilanyloxy)propoxy]-2-[(R)-oxiran-2-yl]ethyl benzoate; With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; at -78 - -30 ℃; for 2.5h; Inert atmosphere;

With water; sodium hydrogencarbonate; In tetrahydrofuran; hexane; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.028