phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside
CAS No.:741677-99-6
Molecular Formula:C₃₆H₄₀O₈S
Molecular Weight:632.775
Hs Code.:

Synonyms:phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Suppliers and Price of phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

There total 9 articles about phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 741677-98-5
phenyl 2,3,4-tri-O-(4-methoxyphenylmethyl)-1-thio-6-O-triphenylmethyl-β-D-galactopyranoside

: 741677-99-6
phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Guidance literature:: With hydrogenchloride; methanol; In methanol; chloroform; at 20 ℃; for 1.5h;
DOI:10.1021/jm0504297

Reference yield: 69.0%

: 1309377-87-4
phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-O-(tertbutyldimethylsiloxypropyl)-1-thio-β-D-galactopyranoside

: 741677-99-6
phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 7h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.023

Reference yield:

: 220774-86-7
phenyl 1-thio-6-O-triphenylmethyl-β-D-galactopyranoside

: 741677-99-6
phenyl 2,3,4-tri-O-(4-methoxybenzyl)-6-hydroxy-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 98 percent / dimethylformamide / 20 °C

2.1: 92 percent / HCl/MeOH / CHCl₃; methanol / 1.5 h / 20 °C

With hydrogenchloride; methanol; sodium hydride; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm0504297