di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide

Base Information

• Chemical Name: di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide
• CAS No.: 923279-01-0
• Molecular Formula: C₂₈H₄₀N₂O₄Se₂
• Molecular Weight: 626.557
• Mol file: 923279-01-0.mol

Synonyms:di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide

Chemical Property of di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide

Chemical Property:

Purity/Quality:

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Technology Process of di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide

There total 6 articles about di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2S)-2-[N-(tert-butoxycarbonyl)amino]-1-iodo-3-phenylpropane (154669-56-4) → di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide (923279-01-0)

Guidance literature:

With sodium selenoborate; In tetrahydrofuran; at 0 ℃; for 0.333333h; Reagent/catalyst; Inert atmosphere;

DOI:10.1039/c5ra06147d

Reference yield: 76.0%

(S)-N-t-butoxycarbonyl-2-phenylmethyl aziridine (153782-96-8) → C14H21NO2Se + di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide (923279-01-0)

Guidance literature:

With bis(trimethylsilyl)selenide; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; regioselective reaction; Inert atmosphere;

DOI:10.1002/adsc.201800602

Reference yield: 75.0%

(S)-N-t-butoxycarbonyl-2-phenylmethyl aziridine (153782-96-8) → di((2S)-2-(t-butoxycarbonylamino)-3-phenylpropyl) diselenide (923279-01-0)

Guidance literature:

With dilithium diselenide; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/ol034773e

upstream raw materials:

(S)-N-t-butoxycarbonyl-2-phenylmethyl aziridine

di-tert-butyl dicarbonate

L-Phenylalaninol

(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol