1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

Base Information

Chemical Name:1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane
CAS No.:791610-23-6
Molecular Formula:C₁₈H₂₀N₂O₄S₂
Molecular Weight:392.5
Hs Code.:

Synonyms:1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

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Chemical Property of 1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

Chemical Property:

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Technology Process of 1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

There total 6 articles about 1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 791610-26-9
1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]-2,2'-dimethylethane

: 791610-23-6
1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

Guidance literature:: 1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]-2,2'-dimethylethane; With naphthalene; sodium; In tetrahydrofuran; at 20 ℃; for 12h;

With hydrogenchloride; Further stages.;
DOI:10.1002/chem.200601167

Reference yield:

: 791610-25-8
1-amino-2-[2,3-di(isopropylmercapto)benzamido]-2-(2,2'-dimethyl)ethane

: 791610-23-6
1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 92 percent / NEt₃ / tetrahydrofuran / 12 h / 20 °C

2.1: naphthalene; sodium / tetrahydrofuran / 12 h / 20 °C

2.2: 96 percent / hydrochloric acid

With naphthalene; sodium; triethylamine; In tetrahydrofuran;
DOI:10.1002/chem.200601167

Reference yield:

: 791610-24-7
1-(tert-butyloxycarbamido)-2-[2,3-di(isopropylmercapto)benzamido]-2,2'-dimethylethane

: 791610-23-6
1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)-2,2'-dimethylethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 64 percent / trifluoroacetic acid / CHCl₃ / 24 h / 20 °C

2.1: 92 percent / NEt₃ / tetrahydrofuran / 12 h / 20 °C

3.1: naphthalene; sodium / tetrahydrofuran / 12 h / 20 °C

3.2: 96 percent / hydrochloric acid

With naphthalene; sodium; triethylamine; trifluoroacetic acid; In tetrahydrofuran; chloroform;
DOI:10.1002/chem.200601167