3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

Base Information

Chemical Name:3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione
CAS No.:1383688-05-8
Molecular Formula:C₃₈H₄₄Br₂N₂O₂
Molecular Weight:720.588
Hs Code.:

Synonyms:3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

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Chemical Property of 3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

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Technology Process of 3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

There total 4 articles about 3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 18908-66-2
3-bromomethylheptane

: 1335131-35-5
3,7-di(4-bromophenyl)-2,6-dioxo-1,2,5,6-tetrahydrobenzo[1,2-b:4,5-b']dipyrrole

: 1383688-05-8
3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

Guidance literature:: With potassium tert-butylate; In 1-methyl-pyrrolidin-2-one; at 60 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc32184j

Reference yield:

: 1335131-33-3
3,7-di(4-bromophenyl)-2,6-dioxo-1,2,3,4,5,6,7-hexahydrobenzo[1,2-b:4,5-b']dipyrrole

: 1383688-05-8
3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium hydroxide / ethanol / 24 h / 20 °C

2: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 24 h / 60 °C / Inert atmosphere

With potassium tert-butylate; dihydrogen peroxide; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol;
DOI:10.1039/c2cc32184j

Reference yield:

: 1335131-32-2
2-(4-Bromo-phenyl)-N-{4-[2-(4-bromo-phenyl)-2-hydroxy-acetylamino]-phenyl}-2-hydroxy-acetamide

: 1383688-05-8
3,7-bis(4-bromophenyl)-1,5-bis(2-ethylhexyl)pyrrolo-[2,3-f]indole-2,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 20 °C

2: dihydrogen peroxide; sodium hydroxide / ethanol / 24 h / 20 °C

3: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 24 h / 60 °C / Inert atmosphere

With sulfuric acid; potassium tert-butylate; dihydrogen peroxide; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol;
DOI:10.1039/c2cc32184j