3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt

Base Information

• Chemical Name: 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt
• CAS No.: 1188410-68-5
• Molecular Formula: C₁₈H₁₄BrClN₂SSe
• Molecular Weight: 484.706

Synonyms:3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt

Chemical Property of 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt

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Technology Process of 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt

There total 1 articles about 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

C11H10BrNS + p-chlorophenyl isoselenocyanate (14223-48-4) → 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt (1188410-68-5)

Guidance literature:

In tetrahydrofuran; at -20 ℃; Inert atmosphere;

DOI:10.1039/b904575a

Reference yield: 76.0%

3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt (1188410-68-5) + Methyl 5-methyl-2,3-hexadienoate (34714-95-9) → (2Z,5Z)-methyl 4-(4-bromobenzylamino)-5-(4-chlorophenylimino)-2-(2-methylpropylidene)-2,5-dihydroselenophene-3-carboxylate (1188410-88-9)

Guidance literature:

In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1039/b904575a

Reference yield: 68.0%

methyl 5-phenyl-2,3-pentadienoate (1006879-10-2) + 3-(4-bromobenzyl)-4-methyl-2-(4-chlorophenyl)selenocarbamoylthiazolium inner salt (1188410-68-5) → (2Z,5Z)-methyl 4-(4-bromobenzylamino)-5-(4-chlorophenylimino)-2-(2-phenylethylidene)-2,5-dihydroselenophene-3-carboxylate (1188410-91-4)

Guidance literature:

In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1039/b904575a

upstream raw materials:

p-chlorophenyl isoselenocyanate

Downstream raw materials:

(2Z,5Z)-methyl 4-(4-bromobenzylamino)-5-(4-chlorophenylimino)-2-(2-phenylethylidene)-2,5-dihydroselenophene-3-carboxylate

(2Z,5Z)-methyl 4-(4-bromobenzylamino)-5-(4-chlorophenylimino)-2-(2-methylpropylidene)-2,5-dihydroselenophene-3-carboxylate

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