p-chlorophenyl isoselenocyanate

Base Information

• Chemical Name: p-chlorophenyl isoselenocyanate
• CAS No.: 14223-48-4
• Molecular Formula: C₇H₄ClNSe
• Molecular Weight: 216.528

Synonyms:p-chlorophenyl isoselenocyanate

Chemical Property of p-chlorophenyl isoselenocyanate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-chlorophenyl isoselenocyanate

There total 8 articles about p-chlorophenyl isoselenocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p-chlorphenylisocyanate (104-12-1) → p-chlorophenyl isoselenocyanate (14223-48-4)

Guidance literature:

With trimethylaluminum; 1,1,1,3,3,3-hexabutyldistannaselenane; In 1,4-dioxane; hexane; toluene; at 100 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.11.069

Reference yield: 72.0%

N-(4-chlorophenyl)formamide (2617-79-0) → p-chlorophenyl isoselenocyanate (14223-48-4)

Guidance literature:

With selenium; bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; Heating;

DOI:10.3987/COM-06-10766

Reference yield: 65.0%

p-chlorophenyl isocyanide (1885-81-0) → p-chlorophenyl isoselenocyanate (14223-48-4)

Guidance literature:

With selenium; triethylamine;

DOI:10.1016/S0040-4020(01)80783-3

upstream raw materials:

carbon diselenide

4-chloro-aniline

N-(4-chlorophenyl)formamide

p-chlorophenyl isocyanide

Downstream raw materials:

C₁₁H₁₂ClNO₂SSe

(4-chloro-phenyl)-selenourea

N-Phenyl-N'-(p-chlor-phenyl)-selenoharnstoff

O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

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