Technology Process of uranium triiodide
There total 17 articles about uranium triiodide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
zinc;
In
neat (no solvent);
byproducts: ZnI2; uranium metal (prewashed with HNO3, H2O and acetone) and iodine (purified by sublimation) and zinc metal are sealed in an evacuated quartz tube and heated at 700°C for 2 d; ZnI2 is separated by sublimation at 450°C, elem. anal.;
DOI:10.1016/0020-1693(94)03898-8
- Guidance literature:
-
In
neat (no solvent);
uranium turnings and HgI in evacuated (1E-6 mbar) ampoule were heated at315°C for 3 + 2 days, heated at 200°C for 2 h, at 300.deg ree.C for 1 h and at 400°C for 30 min;
DOI:10.1016/j.jorganchem.2008.03.030
- Guidance literature:
-
In
diethyl ether;
Sonication; uranium turnings were treated with complex in diethyl ether, stirred for5 days with occasional sonication; filtered, washed with diethyl ether, dried under vac.;
DOI:10.1021/ic801138e
