N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

Base Information

Chemical Name:N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide
CAS No.:1456620-73-7
Molecular Formula:C₂₀H₂₅N₅O₂S
Molecular Weight:399.517
Hs Code.:

Synonyms:N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

Chemical Property:

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Technology Process of N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

There total 3 articles about N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103-72-0
phenyl isothiocyanate

: 204973-87-5
[4-(2-methoxyphenyl)piperazin-1-yl]acetohydrazide

: 1456620-73-7
N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

Guidance literature:: at 100 ℃; for 0.166667h; Temperature; Time; Irradiation; Sealed tube;
DOI:10.1016/j.cclet.2016.12.012

Reference yield:

: 35386-24-4
1-(2-Methoxyphenyl)piperazine

: 1456620-73-7
N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 2 h / 20 °C

2: hydrazine hydrate / ethanol / 9 h / Reflux

3: ethanol / 6 h / Reflux

With hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/j.ejmech.2013.06.045

Reference yield:

: 63854-11-5
ethyl [4-(2-methoxyphenyl)piperazin-1-yl]acetate

: 1456620-73-7
N-phenyl-2-{[4-(2-methoxyphenyl)piperazin-1yl]acetyl}hydrazincarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 9 h / Reflux

2: ethanol / 6 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2013.06.045