Technology Process of C19H29N5O5
There total 3 articles about C19H29N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(2-azidoethoxy)ethanamine hydrochloride;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
4-(2-t-butoxycarbonamidoethyl)phenoxyacetic acid;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1039/c1ob05996c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05996c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C
2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1ob05996c