tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

Base Information

Chemical Name:tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate
CAS No.:1357268-55-3
Molecular Formula:C₁₄H₁₄O₂PS₂*C₂₄H₂₀P
Molecular Weight:648.766
Hs Code.:

Synonyms:tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

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Chemical Property of tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

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Technology Process of tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

There total 3 articles about tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1357268-56-4
C₁₄H₁₅O₂PS₂*H₃N

: 2001-45-8
tetraphenyl phosphonium chloride

: 1357268-55-3
tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

Guidance literature:: In water; for 0.5h;
DOI:10.1039/c1dt11637a

Reference yield:

: 71360-04-8
Bisphosphine oxide

: 1357268-55-3
tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride

2: sulfur / toluene / Inert atmosphere; Reflux

3: water / 0.5 h

With diisobutylaluminium hydride; sulfur; In water; toluene;
DOI:10.1039/c1dt11637a

Reference yield:

: 10177-79-4
bis(2-methoxyphenyl)phosphine

: 1357268-55-3
tetraphenylphosphonium bis(o-methoxyphenyl)dithiophosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur / toluene / Inert atmosphere; Reflux

2: water / 0.5 h

With sulfur; In water; toluene;
DOI:10.1039/c1dt11637a