N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine

Base Information

• Chemical Name: N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine
• CAS No.: 457072-36-5
• Molecular Formula: C₁₈H₂₂N₄
• Molecular Weight: 294.399

Synonyms:N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine

Chemical Property of N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine

Chemical Property:

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Technology Process of N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine

There total 1 articles about N¹,N¹-dimethyl-N²-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

4-amino-6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidine (457072-65-0) + N,N-dimethylbenzamide (611-74-5) → N1,N1-dimethyl-N2-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine (457072-36-5)

Guidance literature:

With triethylamine; trichlorophosphate; In chloroform; for 52h; Reflux;

DOI:10.1002/jhet.1628

Reference yield: 61.0%

N1,N1-dimethyl-N2-(6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidin-4-yl)benzamidine (457072-36-5) → N-[2-(3-phenyl[1,2,4]oxadiazol-5-yl)cyclohepten-1-yl]formamideoxime (457072-07-0)

Guidance literature:

With hydroxylamine hydrochloride; In methanol; at 20 ℃; for 22h;

DOI:10.1002/jhet.1628

upstream raw materials:

4-amino-6,7,8,9-tetrahydro-5H-cyclohepta[1,2-d]pyrimidine

N,N-dimethylbenzamide

Downstream raw materials:

N-[2-(3-phenyl[1,2,4]oxadiazol-5-yl)cyclohepten-1-yl]formamideoxime

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