Benzylaethylphosphinsaeure

Base Information

• Chemical Name: Benzylaethylphosphinsaeure
• CAS No.: 13345-29-4
• Molecular Formula: C₉H₁₃O₂P
• Molecular Weight: 184.175
• Mol file: 13345-29-4.mol

Synonyms:Benzylaethylphosphinsaeure

Chemical Property of Benzylaethylphosphinsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzylaethylphosphinsaeure

There total 3 articles about Benzylaethylphosphinsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

benzaldehyde (100-52-7) + dibenzyl(ethyl)phosphine oxide → (E)-1,2-diphenyl-ethene (103-30-0) + Benzylaethylphosphinsaeure (13345-29-4)

Guidance literature:

dibenzyl(ethyl)phosphine oxide; With sodium amide; In tetrahydrofuran; at 58 - 60 ℃; for 1h;

benzaldehyde; In tetrahydrofuran; for 1h; Heating;

DOI:10.1023/A:1026340532022

Reference yield:

Benzylaethylphosphinsaeureisopropylester (14561-16-1) → Benzylaethylphosphinsaeure (13345-29-4)

Guidance literature:

With hydrogenchloride;

Reference yield:

benzyl chloride (100-44-7) → Benzylaethylphosphinsaeure (13345-29-4)

Guidance literature:

Multi-step reaction with 2 steps

2: HCl

With hydrogenchloride;

upstream raw materials:

Benzylaethylphosphinsaeureisopropylester

benzaldehyde

benzyl chloride

Downstream raw materials:

p-Nitrobenzylaethylphosphinsaeure