C₁₅H₁₄BrNO₃

Base Information

Chemical Name:C₁₅H₁₄BrNO₃
CAS No.:945902-94-3
Molecular Formula:C₁₅H₁₄BrNO₃
Molecular Weight:336.185
Hs Code.:

C<sub>15</sub>H<sub>14</sub>BrNO<sub>3</sub>

Synonyms:C₁₅H₁₄BrNO₃

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Chemical Property of C₁₅H₁₄BrNO₃

Chemical Property:

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Technology Process of C₁₅H₁₄BrNO₃

There total 9 articles about C₁₅H₁₄BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945898-89-5
1,2-dihydro-6-hydroxymethyl-2-oxo-1-phenylpyridine-3-carboxylic acid ethyl ester

: 945902-94-3
C₁₅H₁₄BrNO₃

Guidance literature:: With phosphorus tribromide; In dichloromethane; at -20 ℃; for 4h;

Reference yield:

: 694475-70-2
6-methyl-2-oxo-1-phenyl-1,2-dihydro-3-pyridinecarboxylic acid

: 945902-94-3
C₁₅H₁₄BrNO₃

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Heating / reflux

2: triethylamine / acetonitrile / 2 h / 0 - 20 °C

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / Heating / reflux; Irradiation

4: water; sodium hydrogencarbonate / 1,4-dioxane / 3 h / 60 °C

5: ammonium formate / palladium 10% on activated carbon / ethyl acetate / 8 h / 65 °C

6: phosphorus tribromide / dichloromethane / 4 h / -20 °C

With N-Bromosuccinimide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); water; ammonium formate; phosphorus tribromide; sodium hydrogencarbonate; triethylamine; palladium 10% on activated carbon; N,N-dimethyl-formamide; In 1,4-dioxane; tetrachloromethane; dichloromethane; ethyl acetate; acetonitrile;

Reference yield:

: 945898-86-2
1,2-dihydro-6-methyl-2-oxo-1-phenylpyridine-3-carboxylic acid ethyl ester

: 945902-94-3
C₁₅H₁₄BrNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / Heating / reflux; Irradiation

2: water; sodium hydrogencarbonate / 1,4-dioxane / 3 h / 60 °C

3: ammonium formate / palladium 10% on activated carbon / ethyl acetate / 8 h / 65 °C

4: phosphorus tribromide / dichloromethane / 4 h / -20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; ammonium formate; phosphorus tribromide; sodium hydrogencarbonate; palladium 10% on activated carbon; In 1,4-dioxane; tetrachloromethane; dichloromethane; ethyl acetate;