6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

Base Information

Chemical Name:6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole
CAS No.:151384-96-2
Molecular Formula:C₂₃H₂₄N₂O₅S
Molecular Weight:440.52
Hs Code.:

Synonyms:6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

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Chemical Property of 6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

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Technology Process of 6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

There total 9 articles about 6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 124-63-0
methanesulfonyl chloride

: 151384-95-1
6-benzyloxy-3-hydroxymethyl-1-(N-methyl-2-pyrrolecarboxy)indole

: 151384-96-2
6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 23 ℃; for 1h;

Reference yield:

: 610-78-6
3-nitro-4-chlorophenol

: 151384-96-2
6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

Guidance literature:: Multi-step reaction with 8 steps

1: K₂CO₃, TBAI / acetone / 16 h / Heating

2: dimethylsulfoxide / 24 h / 110 °C

3: DIBAL / tetrahydrofuran / 2 h / 23 °C

4: PtO₂ / ethanol / 6 h / 23 °C

5: pyridine / 1 h / 0 - 23 °C

6: sodium bis(2-methoxyethoxy)aluminum hydride (Red-Al) / toluene / 1 h / 100 °C

7: 48 percent / EDCl / dimethylformamide / 20 h / 23 °C

8: 49 percent / pyridine / dimethylformamide / 1 h / 23 °C

With pyridine; platinum(IV) oxide; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 106014-83-9
2-[4-(benzyloxy)-2-nitrophenyl]propane-1,3-diol

: 151384-96-2
6-benzyloxy-1-(N-methyl-2-pyrrolecarboxy)-3-methanesulfonyloxymethylindole

Guidance literature:: Multi-step reaction with 5 steps

1: PtO₂ / ethanol / 6 h / 23 °C

2: pyridine / 1 h / 0 - 23 °C

3: sodium bis(2-methoxyethoxy)aluminum hydride (Red-Al) / toluene / 1 h / 100 °C

4: 48 percent / EDCl / dimethylformamide / 20 h / 23 °C

5: 49 percent / pyridine / dimethylformamide / 1 h / 23 °C

With pyridine; platinum(IV) oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In ethanol; N,N-dimethyl-formamide; toluene;