1-(chloromethyl)-3,5-diethoxybenzene

Base Information

Chemical Name:1-(chloromethyl)-3,5-diethoxybenzene
CAS No.:1073142-73-0
Molecular Formula:C₁₁H₁₅ClO₂
Molecular Weight:214.692
Hs Code.:
Mol file:1073142-73-0.mol

Synonyms:3,5-diethoxybenzyl chloride

Suppliers and Price of 1-(chloromethyl)-3,5-diethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
1-(chloromethyl)-3,5-diethoxybenzene 95
25g
$ 3245.00

American Custom Chemicals Corporation
1-(CHLOROMETHYL)-3,5-DIETHOXYBENZENE 95.00%
5MG
$ 500.72

Total 1 raw suppliers

Chemical Property of 1-(chloromethyl)-3,5-diethoxybenzene

Chemical Property:

Boiling Point:311.5±27.0 °C(Predicted)
Density:1.083±0.06 g/cm3(Predicted)

Purity/Quality:: 1-(chloromethyl)-3,5-diethoxybenzene 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(chloromethyl)-3,5-diethoxybenzene

There total 3 articles about 1-(chloromethyl)-3,5-diethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 198623-56-2
3,5-diethoxybenzyl alcohol

: 1073142-73-0
3,5-diethoxybenzyl chloride

Guidance literature:: With tetrachloromethane; triphenylphosphine; Heating;
DOI:10.1016/j.bmc.2008.07.086

Reference yield:

: 120355-79-5
3,5-diethoxybenzaldehyde

: 1073142-73-0
3,5-diethoxybenzyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4.5 h / 100 °C

2: thionyl chloride; pyridine / tetrahydrofuran / 8 h / 0 - 20 °C

With pyridine; methanol; sodium tetrahydroborate; thionyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bioorg.2020.104239

Reference yield:

: 26153-38-8
3,5-dihydroxybenzaldehyde

: 1073142-73-0
3,5-diethoxybenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium iodide / acetone / 0.5 h / 50 °C

1.2: 12 h / 80 - 85 °C

2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4.5 h / 100 °C

3.1: thionyl chloride; pyridine / tetrahydrofuran / 8 h / 0 - 20 °C

With pyridine; methanol; sodium tetrahydroborate; thionyl chloride; potassium carbonate; potassium iodide; In tetrahydrofuran; acetone; 1.1: |Williamson Ether Synthesis;
DOI:10.1016/j.bioorg.2020.104239