N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride

Base Information

• Chemical Name: N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride
• CAS No.: 150512-57-5
• Molecular Formula: C₂₉H₃₃Cl₂N₃O₈S₃
• Molecular Weight: 718.7
• Mol file: 150512-57-5.mol

Synonyms:N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride

Chemical Property of N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride

There total 1 articles about N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazundecanedioic acid (110345-42-1) → N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride (150512-57-5)

Guidance literature:

In dichloromethane;

Reference yield: 44.0%

5,8,11-Trioxa-2,14-diazapentadecan (68960-89-4) + N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride (150512-57-5) → 1,13-Dimethyl-4,7,10-tris(p-tolylsulfonyl)-16,19,22-trioxa-1,4,7,10,13-pentaazacyclotetracosane-2,12-dione (110345-41-0)

Guidance literature:

In benzene; for 4h; Ambient temperature;

DOI:10.1007/BF00767393

Reference yield: 28.0%

1-Cyclohexyl-1.2-diaminoethane (150512-62-2) + N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazaundecanedioic acid dichloride (150512-57-5) → 5-Cyclohexyl-1,10,13-Tris(p-toluenesulfonyl)-1,4,7,10,13-pentaazacyclopenta-decan-3,8-dione (150512-63-3)

Guidance literature:

In dichloromethane;

upstream raw materials:

N,N',N-Tris(p-tolylsulfonyl)-3,6,9-triazundecanedioic acid

Downstream raw materials:

1,13-Dimethyl-4,7,10-tris(p-tolylsulfonyl)-16-oxa-1,4,7,10,13-pentaazacyclooctadecane-1,12-dione

1,13-Dimethyl-4,7,10-tris(p-tolylsulfonyl)-16,19,22-trioxa-1,4,7,10,13-pentaazacyclotetracosane-2,12-dione

5-Cyclohexyl-1,10,13-Tris(p-toluenesulfonyl)-1,4,7,10,13-pentaazacyclopenta-decan-3,8-dione