(2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate

Base Information

• Chemical Name: (2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate
• CAS No.: 1193305-89-3
• Molecular Formula: C₁₈H₂₈O₄
• Molecular Weight: 308.418
• Mol file: 1193305-89-3.mol

Synonyms:(2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate

Chemical Property of (2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate

There total 1 articles about (2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

(2R,4R)-2-(benzyloxy)nonane-1,4-diol (1193305-88-2) + acetyl chloride (75-36-5) → (2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate (1193305-89-3)

Guidance literature:

With 2,3,5-trimethyl-pyridine; In dichloromethane; at -78 - -40 ℃; for 9h; Inert atmosphere;

DOI:10.1016/j.tet.2009.08.054

Reference yield: 93.0%

(2R,4R)-2-(benzyloxy)-4-hydroxynonyl acetate (1193305-89-3) + tert-butylchlorodiphenylsilane (58479-61-1) → (2R,4R)-2-(benzyloxy)-4-(tert-butyldiphenylsilyl-oxy)nonyl acetate (1193305-90-6)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tet.2009.08.054

upstream raw materials:

(2R,4R)-2-(benzyloxy)nonane-1,4-diol

acetyl chloride

Downstream raw materials:

(2R,4R)-2-(benzyloxy)-4-(tert-butyldiphenylsilyl-oxy)nonyl acetate