diethyl(2,6-dimethoxyphenyl)phosphite

Base Information

Chemical Name:diethyl(2,6-dimethoxyphenyl)phosphite
CAS No.:247052-35-3
Molecular Formula:C₁₂H₁₉O₄P
Molecular Weight:258.254
Hs Code.:

Synonyms:diethyl(2,6-dimethoxyphenyl)phosphite

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Chemical Property of diethyl(2,6-dimethoxyphenyl)phosphite

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Technology Process of diethyl(2,6-dimethoxyphenyl)phosphite

There total 1 articles about diethyl(2,6-dimethoxyphenyl)phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-57-1
diethyl phosphorylchloridite

: 151-10-0
1,3-Dimethoxybenzene

: 247052-35-3
diethyl(2,6-dimethoxyphenyl)phosphite

Guidance literature:: 1,3-Dimethoxybenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at 20 ℃; for 4h;

diethyl phosphorylchloridite; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0022-328X(99)00210-7

Reference yield: 55.0%

: 247052-35-3
diethyl(2,6-dimethoxyphenyl)phosphite

: 126590-36-1
2,6-(dimethoxyphenyl)phosphine

Guidance literature:: With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; at 0 ℃; for 6h;
DOI:10.1016/S0022-328X(99)00210-7

Reference yield:

: 247052-35-3
diethyl(2,6-dimethoxyphenyl)phosphite

: 247052-36-4
2,6-dimethoxyphenylphosphetane

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / LiAlH₄; Me₃SiCl / tetrahydrofuran / 6 h / 0 °C

2: 86 percent / n-BuLi / tetrahydrofuran / 1 h / 0 °C

With lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; In tetrahydrofuran; 1: Reduction / 2: Cyclization;
DOI:10.1016/S0022-328X(99)00210-7