N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

Base Information

Chemical Name:N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone
CAS No.:212608-90-7
Molecular Formula:C₃₅H₃₄N₂O₉
Molecular Weight:626.663
Hs Code.:

N<sup>1</sup>-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

Synonyms:N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

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Technology Process of N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

There total 3 articles about N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 208931-58-2
1-(4-Hydroxy-butyl)-3-methyl-1H-pyrazin-2-one

: 212608-90-7
N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

Guidance literature:: With tin(IV) chloride; In acetonitrile; at 0 ℃;
DOI:10.1080/07328319808003482

Reference yield:

: 19838-07-4
3-methylpyrazin-2(1H)-one

: 212608-90-7
N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: MeONa / methanol

3: 45 percent / SnCl₄ / acetonitrile / 0 °C

With sodium methylate; tin(IV) chloride; sodium hydride; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/07328319808003482

Reference yield:

: 208931-55-9
Acetic acid 4-(3-methyl-2-oxo-2H-pyrazin-1-yl)-butyl ester

: 212608-90-7
N¹-[4-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyloxy)-butyl]-3-methyl-2-pyrazinone

Guidance literature:: Multi-step reaction with 2 steps

1: MeONa / methanol

2: 45 percent / SnCl₄ / acetonitrile / 0 °C

With sodium methylate; tin(IV) chloride; In methanol; acetonitrile;
DOI:10.1080/07328319808003482