hexachlorodigermane

Base Information

• Chemical Name: hexachlorodigermane
• CAS No.: 15432-44-7
• Molecular Formula: Cl₆Ge₂
• Molecular Weight: 357.898
• Mol file: 15432-44-7.mol

Synonyms:hexachlorodigermane

Chemical Property of hexachlorodigermane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of hexachlorodigermane

There total 2 articles about hexachlorodigermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

germanium(II) chloride dioxane + 1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene (153625-67-3) → hexachlorodigermane (15432-44-7) + (1,2-bis((2,6-diisopropylphenyl)imino)acenaphthene(1-))GeCl (812645-94-6)

Guidance literature:

In diethyl ether; under vac. using Schlenk ampules; Ge complex added to a suspn. of ligand, shaken at room temp.; filtered, concd. (vac.), crystd. for 2 d; elem. anal.;

DOI:10.1021/ic048801g

Reference yield:

germanium subchloride → hexachlorodigermane (15432-44-7) + germaniumtetrachloride (10038-98-9)

Guidance literature:

In neat (no solvent); thermal decompn. of very pure (GeCl)x at 210 °C in vac. (0.05-0.1 torr);; soln. of Ge2Cl6 in GeCl4, sepn. by vac. distillation at -30 °C;;

upstream raw materials:

1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene