Technology Process of C30H38O4Si
There total 10 articles about C30H38O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
2: toluene-4-sulfonic acid
3: copper(l) iodide; potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 20 °C
4: methanol / dichloromethane / 20 °C
5: quinoline; hydrogen / ethyl acetate / 20 °C
6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
7: toluene / 2 h / Reflux
With
quinoline; methanol; copper(l) iodide; oxalyl dichloride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; sodium iodide;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
1: Jones oxidation / 5: Lindlar hydrogenation / 6: Swern oxidation / 7: Wittig homologation;
DOI:10.1016/j.tetlet.2012.01.032
- Guidance literature:
-
Multi-step reaction with 6 steps
1: toluene-4-sulfonic acid
2: copper(l) iodide; potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 20 °C
3: methanol / dichloromethane / 20 °C
4: quinoline; hydrogen / ethyl acetate / 20 °C
5: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
6: toluene / 2 h / Reflux
With
quinoline; methanol; copper(l) iodide; oxalyl dichloride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; sodium iodide;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
4: Lindlar hydrogenation / 5: Swern oxidation / 6: Wittig homologation;
DOI:10.1016/j.tetlet.2012.01.032
