1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

Base Information

Chemical Name:1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide
CAS No.:1203477-59-1
Molecular Formula:Br*C₂₃H₂₉N₄
Molecular Weight:441.414
Hs Code.:

Synonyms:1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

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Technology Process of 1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

There total 1 articles about 1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 123-75-1
pyrrolidine

: 1203477-57-9
3-{[6-(bromomethyl)pyridin-2-yl]methyl}-1-mesityl-1H-imidazol-3-ium bromide

: 1203477-59-1
1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

Guidance literature:: With sodium carbonate; In acetone; at 20 ℃; for 12h;
DOI:10.1021/om900894k

Reference yield: 75.0%

: 157072-60-1,61521-25-3,166941-05-5,16971-33-8
(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)

: 1203477-59-1
1-mesityl-3-{[6-(amine-1-ylmethyl)-pyridin-2-yl]methyl}-2,3-dihydro-1H-imidazol-3-ium bromide

: [Ru(H)Cl(CO)(2-[(3-mesityl-2,3-dihydro-1H-imidazol-1-yl)methyl]-6-(pyrrolidin-1-ylmethyl)pyridine)]

Guidance literature:: With K(Me₃SiNSiMe₃); In tetrahydrofuran; under N2; soln. of imidazolium salt and Ru complex in THF stirred at reflux overnight; soln. filtered; solvent removed in vac.; washed with Et2O; taken up in dry THF; soln. of K(Me3SiNSiMe3) in toluene added; stirredfor 2 h; filtered; evapd.; dissolved in CH2Cl2; pptd. with Et2O; elem. anal.;
DOI:10.1021/om101179a