HU 914

Base Information

• Chemical Name: HU 914
• CAS No.: 1309372-88-0
• Molecular Formula: C₂₇H₄₀O₄
• Molecular Weight: 428.612
• Mol file: 1309372-88-0.mol

Synonyms:HU 914

Chemical Property of HU 914

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HU 914

There total 11 articles about HU 914 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

→ HU 914 (1309372-88-0)

Guidance literature:

Reference yield:

HU 912 (1309372-78-8) → HU 914 (1309372-88-0)

Guidance literature:

With potassium tert-butylate; water; In 2-methyltetrahydrofuran; Reagent/catalyst; Solvent; Reflux;

Reference yield:

(Z)-1,3-dimethoxy-5-(2-methyloct-3-en-2-yl)benzene → HU 914 (1309372-88-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 18 h / 30 °C / 3000.3 Torr

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.08 h / 15 °C / Large scale

2.2: 1.33 h / 15 °C / Large scale

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; hexane / 0.25 h / 15 °C / Large scale

3.2: 15 - 25 °C / Large scale

4.1: potassium tert-butylate; water / 2-methyltetrahydrofuran / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; potassium tert-butylate; water; hydrogen; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane; ethyl acetate; 3.1: |Negishi Coupling / 3.2: |Negishi Coupling;

upstream raw materials:

α,α-dimethyl-3,5-dimethoxyphenylacetonitrile

2-(3,5-dimethoxyphenyl)-2-methylpropanal

(1S)-(+)-ketopinic acid

(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptane-1-carboxylic acid methylester

Downstream raw materials:

HU 910