(+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol

Base Information

• Chemical Name: (+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol
• CAS No.: 467471-33-6
• Molecular Formula: C₂₁H₃₀N₂O₂S
• Molecular Weight: 374.547

Synonyms:(+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol

Chemical Property of (+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol

Chemical Property:

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Technology Process of (+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol

There total 1 articles about (+)-(2S,3R,S_S)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methyl [(4S,5R,SS)-4-methyl-2-phenyl-5-(i-propyl)-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl] carboxylate → (+)-(2S,3R,SS)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol (467471-33-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 15h;

DOI:10.1002/chem.200204674

Reference yield: 80.0%

(+)-(2S,3R,SS)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol (467471-33-6) → (-)-(2S,3R)-3-amino-2-(benzylamino)-2,4-dimethylpentan-1-ol (467471-48-3)

Guidance literature:

With trifluoroacetic acid; In methanol; for 7h; Heating;

DOI:10.1002/chem.200204674

Reference yield: 75.0%

tert-butyldimethylsilyl chloride (18162-48-6) + (+)-(2S,3R,SS)-2-(benzylamino)-2,4-dimethyl-3-(p-tolylsulfinylamino)pentan-1-ol (467471-33-6) → (+)-(1R,2S,SS)-N-[2-benzylamino-3-(t-butyldimethylsilyloxy)-2-methyl-1-(isopropyl)prop-1-yl]-p-tolylsulfinamide

Guidance literature:

With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo052077h

Downstream raw materials:

(-)-(2S,3R)-3-amino-2-(benzylamino)-2,4-dimethylpentan-1-ol

((4S,5R)-3-Benzyl-5-isopropyl-4-methyl-4,5-dihydro-3H-imidazol-4-yl)-methanol

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