3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate

Base Information

• Chemical Name: 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate
• CAS No.: 1026928-71-1
• Molecular Formula: C₂₇H₃₀BrN₃O₅S
• Molecular Weight: 588.522

Synonyms:3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate

Chemical Property of 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate

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Technology Process of 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate

There total 1 articles about 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-N-{4-[(piperidin-4-ylamino)sulfonyl]-1-naphthyl}benzamide hydrochloride + 3-bromopropylcarbonochloridate (98829-71-1) → 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate (1026928-71-1)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 4h;

DOI:10.1021/jm061118e

Reference yield:

2,6-dimethyl morpholine (141-91-3) + 3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate (1026928-71-1) → C33H42N4O6S

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 12h;

DOI:10.1021/jm061118e

Reference yield:

3-bromopropyl 4-(1-(2-methylbenzamido)naphthalene-4-sulfonamido)piperidine-1-carboxylate (1026928-71-1) + 1,2,3,4-tetrahydroisoquinoline (91-21-4) → C36H40N4O5S

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 12h;

DOI:10.1021/jm061118e

upstream raw materials:

3-bromopropylcarbonochloridate

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