3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

Base Information

Chemical Name:3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester
CAS No.:1011263-86-7
Molecular Formula:C₁₈H₁₇F₃O₅S
Molecular Weight:402.391
Hs Code.:

Synonyms:3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

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Chemical Property of 3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

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Technology Process of 3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

There total 3 articles about 3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1011263-85-6
3-ethyl-4-hydroxy-5-methyl-benzoic acid benzyl ester

: 358-23-6
trifluoromethylsulfonic anhydride

: 1011263-86-7
3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1011264-26-8
3-ethyl-4-hydroxy-5-methylbenzoic acid

: 1011263-86-7
3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 50 °C

2: pyridine / dichloromethane / 2 h / 0 - 20 °C

With pyridine; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 42900-98-1
3-ethyl-4-hydroxy-5-methylbenzaldehyde

: 1011263-86-7
3-ethyl-5-methyl-4-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium chlorite; sodium dihydrogenphosphate / water; dimethyl sulfoxide / 25 h / 20 - 40 °C / Exothermic; Cooling with ice-bath

1.2: pH 2 - 3

2.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 50 °C

3.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

With pyridine; sodium chlorite; sodium dihydrogenphosphate; potassium hydrogencarbonate; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;