phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

Base Information

Chemical Name:phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside
CAS No.:1447801-66-2
Molecular Formula:C₃₃H₃₄O₉S
Molecular Weight:606.694
Hs Code.:

Synonyms:phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

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Technology Process of phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

There total 2 articles about phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 175978-43-5
phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

: 1447801-66-2
phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo400467g

Reference yield:

: 1276114-16-9
C₄₇H₅₀O₈SSi

: 1447801-66-2
phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrogenfluoride / tetrahydrofuran / 0 - 20 °C

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo400467g

Reference yield: 52.0%

: 1276114-12-5
4-((benzyl(5-hydroxypentyl)carbamoyloxy)methyl)benzyl benzoate

: 1447801-66-2
phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

: 1447801-93-5
4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo400467g