4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

Base Information

Chemical Name:4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate
CAS No.:1447801-93-5
Molecular Formula:C₅₅H₅₉NO₁₄
Molecular Weight:958.072
Hs Code.:

Synonyms:4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

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Chemical Property of 4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

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Technology Process of 4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

There total 3 articles about 4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1276114-12-5
4-((benzyl(5-hydroxypentyl)carbamoyloxy)methyl)benzyl benzoate

: 1447801-66-2
phenyl 6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

: 1447801-93-5
4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo400467g

Reference yield:

: 1276114-16-9
C₄₇H₅₀O₈SSi

: 1447801-93-5
4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine hydrogenfluoride / tetrahydrofuran / 0 - 20 °C

2: pyridine / dichloromethane / 0 - 20 °C

3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / -20 - 20 °C / Inert atmosphere

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo400467g

Reference yield:

: 175978-43-5
phenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-1-thio-α-L-idopyranoside

: 1447801-93-5
4-[(phenylcarboxy)methyl]benzyl N-benzyl-N-[5-((6-O-acetyl-2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-α-L-idopyranosyl)oxy)pentyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / -20 - 20 °C / Inert atmosphere

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane;
DOI:10.1021/jo400467g